Chemically Induced Dynamic Nuclear and Electron Polarizations-Cidnp and Cidep
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Chemically Induced Dynamic Nuclear and Electron Polarizations-Cidnp and Cidep

Chemically Induced Dynamic Nuclear and Electron Polarizations-Cidnp and Cidep


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About the Book

Anomalous electron-spin state populations in the Electron Paramagnetic Re- sonance (EPR) spectra of radicals formed during radio lysis experiments were observed in 1963 by FESSENDEN and SCHULER [170a]. This phenomenon did not receive much attention at the time. In 1967, BARGON, FISCHER, and JOHNSEN [5] and independently WARD and LAWLER [7,8] reported a similar phenomenon for Nuclear Magnetic Resonance (NMR) spectra taken during radical reactions: emission or enhanced absorption, or both. The earliest attempts to explain this new NMR phenomenon treated these effects in a way similar to that of Dynamic Nuclear Polarization (DNP) or the Overhauser effect. Although the polarization has a completely different origin, DNP gave its name to this effect: Chemically Induced Dynamic Nuclear Polariza- tion (CIDNP). [The name Chemically Induced Dynamic Electron Polarization (CIDEP) was introduced later by analogy with CIDNP]. After the initial publica- tions, all the new data demonstrated that the first theory could not be correct. In 1969, a new theory was proposed by CLOSS [18] and independently by KAPTEIN and OOSTERHOFF [23] and called the radical-pair theory. This mechanism was proposed to account for the observations of polarization in both NMR and EPR. The radical-pair theory is based on weak interactions in a pair of radicals: the strength of interaction between the electronic states of the radicals depends in particular on the nuclear-spin states.


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Product Details
  • ISBN-13: 9783642657955
  • Publisher: Springer-Verlag Berlin and Heidelberg GmbH & Co. KG
  • Binding: Paperback
  • Height: 244 mm
  • No of Pages: 130
  • Series Title: NMR Basic Principles and Progress
  • Weight: 277 gr
  • ISBN-10: 3642657958
  • Publisher Date: 15 Nov 2011
  • Edition: Softcover reprint of the original 1st ed. 1974
  • Language: English
  • Returnable: Y
  • Spine Width: 7 mm
  • Width: 170 mm


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