Lokale Strukturen nanoskopischer Aluminiumalkoxidfluoride und chemisch verwandter kristalliner Verbindungen
Lokale Strukturen nanoskopischer Aluminiumalkoxidfluoride und chemisch verwandter kristalliner Verbindungen

Lokale Strukturen nanoskopischer Aluminiumalkoxidfluoride und chemisch verwandter kristalliner Verbindungen


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About the Book

In der vorliegenden Promotionsarbeit werden Aluminiumisopropoxidfluoride und verwandte kristalline und amorphe Verbindungen unter Nutzung von NMR-Experimenten untersucht. Die Aufklärung lokaler Strukturen in diesen Materialien bildet ein Bindeglied zwischen der Klärung lokaler Strukturen im high surface-Aluminiumfluorid, das wegen seiner außergewöhnlichen Eigenschaften Gegenstand aktueller Arbeiten ist, und mechanistischen Aspekten der Sol-Gel Fluorolyse von Aluminiumalkoxiden. In drei Kapiteln werden Lösungsansätze zum Nachweis, der Identifikation und Aufklärung lokaler Strukturen in Aluminiumisopropoxidfluoriden vorgestellt: 1. Die Synthese einer Reihe von kristallinen Referenzphasen, 2. Das Verfolgen von Veränderungen lokaler Strukturen in Alkogelen und festen Aluminiumisopropoxidfluoriden mit unterschiedlichem Fluorierungsgrad und 3. Die einfache Variation von Syntheseparametern der Sol-Gel-Synthese. Auf der Basis der vorgestellten Resultate wird ein möglicher Reaktionspfad der Fluorolyse von Aluminiumisopropoxid entwickelt und Strukturmodelle für Zwischenstufen vorgeschlagen.
About the Author: René König wurde am 23.07.1978 in Zeitz, Sachsen-Anhalt, geboren. Nach dem Abitur und einer Ausbildung zum Chemikanten bei der BASF SE, Ludwigshafen, studierte er Chemie an der Humboldt-Universität zu Berlin. Im Juli 2006 schloss René König das Chemie-Studium mit einer Diplomarbeit im Bereich Festkörperchemie an der Humboldt-Universität zu Berlin ab (PD Dr. G. Scholz, Prof. Dr. E. Kemnitz). Thema der Arbeit waren "Magnetresonanzuntersuchungen zur Ausbildung lokaler Strukturen bei der Sol-Gel-Synthese von Aluminiumalkoxidfluorid". Anschließend promovierte er im gleichen Gebiet, die Promotion wurde im August 2009 erfolgreich abgeschlossen. Weiterhin erschienen bisher 8 Veröffentlichungen in angesehenen Fachzeitschriften. Zur Zeit lebt René König mit Frau und Kind in Berlin.


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Product Details
  • ISBN-13: 9783942109000
  • Publisher: Disserta Verlag
  • Publisher Imprint: Disserta Verlag
  • Height: 229 mm
  • No of Pages: 256
  • Spine Width: 16 mm
  • Width: 152 mm
  • ISBN-10: 394210900X
  • Publisher Date: 08 Dec 2009
  • Binding: Hardback
  • Language: German
  • Returnable: N
  • Weight: 562 gr


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