Magnetically and Capillary Driven Grain Boundary Motion in Zinc Bicrystals
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Magnetically and Capillary Driven Grain Boundary Motion in Zinc Bicrystals

Magnetically and Capillary Driven Grain Boundary Motion in Zinc Bicrystals


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About the Book

In der vorliegenden Dissertation wurden neue Erkenntnisse auf dem Gebiet der experimentellen Erforschung der Korngrenzenbewegung vorgestellt. Im Rahmen der Arbeit wurde anhand von in-situ Messungen mittels einer eigens dazu entwickelten Polarisationsmikroskopiesonde mit integriertem Heiztisch die Abhangigkeit der Korngrenzenbeweglichkeit vom Desorientierungs- und Inklinationswinkel der Korngrenze, sowie der Temperatur an speziell gezuchteten Bikristallen aus 99,995% Zink mit symmetrischen und asymmetrischen Kippkorngrenzen und gemischten Korngrenzen im Temperaturbereich zwischen 330°C und 415°C in Hochmagnetfeldern von 10 bis 28 Tesla Starke als Triebkraft untersucht. Dabei wurde die jeweilige Wanderungsgeschwindigkeit v der Korngrenzen bei verschiedenen Temperaturen und treibenden Kraften gemessen. Aus den so erhaltenen Messdaten wurden die Aktivierungsparameter der Korngrenzenbewegung fur die jeweils untersuchte Korngrenze bestimmt.Weiter wurde im Rahmen der Experimente in Hochfeldmagneten gezeigt, dass die Polarisationsmikroskopiesonde zur Bestimmung der Korngrenzenenergie in magnetisch anisotropen Metallen verwendet werden kann. Zu kleinerem Anteil wurden auch Versuche zu krummungsgetriebener Korngrenzenbewegung durchgefuhrt. Alle Ergebnisse zeigten eine starke Inklinations- und Desorientierungsabhangigkeit der Korngrenzenbeweglichkeit, wobei fur asymmetrische Korngrenzen hohere Aktivierungsparameter ermittelt wurden als fur symmetrische. Dies wurde auf Unterschiede zwischen der atomistischen Struktur von asymmetrischen und symmetrischen Korngrenzen zuruckgefuhrt. Weiterhin wurde auch die Auswirkung einer Gluhung im Hochmagnetfeld auf Textur- und Mikrostrukturentwicklung von Zinkpolykristallen untersucht, wobei gezeigt wurde, dass das Magnetfeld ein geeignetes Werkzeug zur Beeinflussung der Mikrostruktur in Zink ist.


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Product Details
  • ISBN-13: 9783954044313
  • Publisher: Na
  • Height: 210 mm
  • Weight: 10 gr
  • ISBN-10: 3954044315
  • Binding: Paperback
  • Language: English
  • Width: 232 mm


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Magnetically and Capillary Driven Grain Boundary Motion in Zinc Bicrystals
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